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. 2019 Mar 7;4(3):5012–5018. doi: 10.1021/acsomega.8b03551

Table 2. Substrate Scope for Mitsunobu Esterification Mediated by PhNO and Ph3Pa.

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a

Conditions: 1a (0.60 mmol), 2a (0.72 mmol), PhNO (1.5 mmol), Ph3P (1.5 mmol), acetonitrile (64 mL); reaction time: 30 min; 0 °C.

b

Determined by 1H NMR. Average of two experiments.

c

Inversion/retention of configuration; determined by high-performance liquid chromatography.