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. Author manuscript; available in PMC: 2020 Aug 15.
Published in final edited form as: Int J Pharm. 2019 Jun 25;567:118470. doi: 10.1016/j.ijpharm.2019.118470

Table S2:

Tg analysis for formulations produced by spray-drying for lyophilization (mean ± SD).

Sample Tg or Tm Lyo (°C)* Tg or Tm SD (°C)*
Lysozyme/Suc 65.6 ± 0.3 68.1 ± 0.1
Lysozyme/Tre 95.1 ± 0.9 103.7 ± 0.6
Lysozyme/Mann 160.6 ± 0.1 163.4 ± 0.1
BSA/Suc 79.8 ± 0.4 80.4 ± 0.1
BSA/Tre 109.2 ± 1.7 116.1 ± 3.3
BSA/Mann 159.5 ± 0.4 161.8 ± 0.2
Myoglobin/Suc 70.0 ± 0.1 65.2 ± 0.5
Myoglobin/Tre 106.6 ± 0.1 105.9 ± 0.7
Myoglobin/Mann 160.1 ± 0.1 160.9 ±0.4
β-Lactoglobulin/Suc 71.8 ± 0.3 72.0 ± 1.3
β-Lactoglobulin/Tre 106.5 ± 0.2 108.4 ± 0.7
β-Lactoglobulin/Mann 160.4 ± 0.4 163.1 ± 0.1
*

Tg for sucrose- and trehalose-containing formulations. Tm for mannitol-containing formulations.