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. 2019 Jul 2;24(13):2439. doi: 10.3390/molecules24132439

Table 1.

2D-heteronuclear multiple quantum coherence (HMQC) correlation of 13C nuclear magnetic resonance (NMR) and 1H-NMR signals for pyrogallol derivative.

Carbon Chemical Shift (ppm) 1H-NMR Signal
13C-NMR 1H-NMR
a 14.271 0.873 t, 3H
b 22.766 1.225–1.307 m, 2H
c 25.809 m, 2H
d 29.303 m, 2H
l 31.712 m, 2H
m 29.773 m, 2H
n 29.533 m, 2H
o 27.373 m, 2H
p 25.127 m, 2H
e 27.373 2.025 q, 2H
k 27.373 q, 2H
q 34.303 2.290 t, 2H
f 128.092 5.288–5.383 m, 1H
g 128.227 m, 1H
h 130.242 m, 1H
i 130.415 m, 1H
r 174.656 No proton -
s 51.696 3.653 s, 3H
u 108.175 6.435 d, 1H
w d, 1H
y 144.362 No proton -
v 120.308 6.634 t, 1H
j 58.742 3.682–3.724 q, 1H
x Not detected Not detected s, OH
t s, OH