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. 2019 Jul 25;10:3316. doi: 10.1038/s41467-019-11326-2

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© The Author(s) 2019

Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license, and indicate if changes were made. The images or other third party material in this article are included in the article’s Creative Commons license, unless indicated otherwise in a credit line to the material. If material is not included in the article’s Creative Commons license and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this license, visit http://creativecommons.org/licenses/by/4.0/.

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Fig. 2 — Importance of data completeness. Small section of the ZSM-5 framework (Grey-red bars: T–O bonds) shows that incomplete data lead to elongated electrostatic potential maps. a 100% complete data. b Missing wedge with 10° opening, 90% data completeness. c Missing wedge with 30° opening, 66% data completeness. d Missing wedge with 50° opening, 45% data completeness. e–h illustration of the missing volume in reciprocal space. Grey: observed data, white wedge: missing data. Green arrow: crystallographic b axis, blue arrow: c axis