Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C11H9IN2OS |
| M r | 344.16 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 298 |
| a, b, c (Å) | 17.4130 (6), 7.5325 (3), 18.5443 (6) |
| β (°) | 94.567 (1) |
| V (Å3) | 2424.61 (15) |
| Z | 8 |
| Radiation type | Mo Kα |
| μ (mm−1) | 2.79 |
| Crystal size (mm) | 0.30 × 0.27 × 0.09 |
| Data collection | |
| Diffractometer | Bruker D8 Venture κ-geometry diffractometer 208039-01 |
| Absorption correction | Multi-scan (SADABS; Krause et al., 2015 ▸) |
| T min, T max | 0.595, 0.745 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 21512, 4448, 3987 |
| R int | 0.020 |
| (sin θ/λ)max (Å−1) | 0.604 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.029, 0.073, 1.12 |
| No. of reflections | 4448 |
| No. of parameters | 297 |
| No. of restraints | 2 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.97, −0.49 |