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. 2019 May 3;75(Pt 6):711–713. doi: 10.1107/S205698901900567X

Table 2. Experimental details.

Crystal data
Chemical formula C23H34N2O4
M r 402.52
Crystal system, space group Orthorhombic, F d d d
Temperature (K) 296
a, b, c (Å) 14.358 (6), 17.333 (7), 38.902 (19)
V3) 9681 (7)
Z 16
Radiation type Mo Kα
μ (mm−1) 0.08
Crystal size (mm) 0.32 × 0.28 × 0.26
 
Data collection
Diffractometer Bruker SMART CCD area detector
Absorption correction Multi-scan (SADABS; Bruker, 2001)
T min, T max 0.822, 1.000
No. of measured, independent and observed [I > 2σ(I)] reflections 11878, 2156, 1501
R int 0.031
(sin θ/λ)max−1) 0.595
 
Refinement
R[F 2 > 2σ(F 2)], wR(F 2), S 0.081, 0.278, 1.05
No. of reflections 2156
No. of parameters 134
No. of restraints 2
H-atom treatment H-atom parameters constrained
Δρmax, Δρmin (e Å−3) 0.38, −0.34

Computer programs: SMART and SAINT (Bruker, 2001), SHELXS (Sheldrick, 2008), SHELXL (Sheldrick, 2015) and OLEX2 (Dolomanov et al., 2009).