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Summary of Silylation Results with Experimental Method
| silica type | silane | % silanol functionalized (IR) | mass % silane (TGA) | mass % sulfur (TSA) |
|---|---|---|---|---|
| silica B | MPTMS | 38 | 10.6 | 3.99 |
| silica A | S4 | 54 | 12.0 | 4.53 |
| silica B | S4 | 17 | 11.0 | 3.98 |
| Ludox | S4 | NA | 4.7 | 1.56 |
