Skip to main content
. Author manuscript; available in PMC: 2020 Jun 5.
Published in final edited form as: J Am Chem Soc. 2019 May 13;141(22):8798–8806. doi: 10.1021/jacs.9b00045

Scheme 1.

Scheme 1.

Syntheses of FAHFA-based standards using iterative, modified Steglich esterification reactionsa

aDMAP: 4-dimethylaminopyridine, EDC: i-ethyl-3-(3-dimethylaminopropyl)carbodiimide, PAHSA: palmitic acid ester of hydroxy stearic acid, POHSA: palmitoleic acid ester of hydroxy stearic acid, OAHSA: oleic acid ester of hydroxy stearic acid.