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. 2019 Jul 31;9:11082. doi: 10.1038/s41598-019-47507-8

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© The Author(s) 2019

Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license, and indicate if changes were made. The images or other third party material in this article are included in the article’s Creative Commons license, unless indicated otherwise in a credit line to the material. If material is not included in the article’s Creative Commons license and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this license, visit http://creativecommons.org/licenses/by/4.0/.

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¹⁵N R_1ρ relaxation dispersion profiles for GB1 in complex with IgG. Experiments were acquired at 700 MHz (16.4 T) with 2 mM Gd(DTPA-BMA) and 850 MHz (20 T) with 5 mM Gd(DTPA-BMA), and a sample temperature of 300 ± 2 K. Best fit curves to a two-site exchange model assuming a common motion are shown as orange lines (k_ex = 13 ± 3 × 10³ s⁻¹). Residue specific φ_ex (×10³ rad² s⁻²) and R_1ρ,0 (s⁻¹) are indicated in each plot.