Skip to main content
. Author manuscript; available in PMC: 2020 Jun 1.
Published in final edited form as: Phytochem Lett. 2019 Apr 6;31:140–146. doi: 10.1016/j.phytol.2019.03.015

Table 2.

13C-NMR chemical shifts for 14, 6 and 11 (in CDCl3, 150 MHz)a

position 1 2 3 4 6 11
1 39.61 38.59 38.65 38.36 39.64 38.64
2 34.09 27.38 27.33 27.02 34.18 27.37
3 217.69 78.90 78.86 76.80 218.13 78.91
4 47.25 38.86 38.83 41.89 47.35 38.85
5 54.86 55.28 55.21 49.90 54.95 55.24
6 19.64 18.28 18.22 18.44 19.70 18.28
7 33.62 34.28 34.20 34.04 33.59 34.17
8 40.65 40.65 40.67 40.82 40.81 40.72
9 49.83 50.36 50.31 50.36 49.82 50.25
10 36.86 37.20 37.15 37.04 36.91 37.16
11 21.50 20.96 20.75 21.37 21.50 20.89
12 25.15 27.27 27.51 26.62 25.18 27.31
13 37.73 36.63 37.24 37.95 38.20 37.01
14 41.93 41.80 42.29 42.80 42.92 42.66
15 26.86 26.79 28.98 27.39 27.45 27.17
16 33.13 32.85 28.73 35.43 35.54 34.96
17 80.17 80.29 59.27 43.00 43.02 43.05
18 48.30 49.17 47.97 48.85 48.27 49.68
19 48.03 52.25 51.06 43.79 47.98 52.61
20 149.64 212.20 211.78 154.73 150.59 212.91
21 29.39 27.55 27.64 31.75 29.86 27.64
22 38.47 38.70 32.42 39.83 39.99 39.84
23 26.63 27.99 27.96 72.11 26.67 27.97
24 21.00 15.38 15.36 11.23 21.05 15.37
25 16.04 16.17 16.13 16.46 15.98 16.07
26 15.90 16.03 15.82 16.00 15.81 15.90
27 13.76 13.17 14.23 14.56 14.50 14.46
28 206.08 17.70 18.03 17.97
29 109.65 29.94 30.23 106.82 109.40 29.17
30 19.28 65.01 19.33
a

The assignments were based on 1H-1H COSY, HMQC and HMBC experiments.