Table 2.
position | 1 | 2 | 3 | 4 | 6 | 11 |
---|---|---|---|---|---|---|
1 | 39.61 | 38.59 | 38.65 | 38.36 | 39.64 | 38.64 |
2 | 34.09 | 27.38 | 27.33 | 27.02 | 34.18 | 27.37 |
3 | 217.69 | 78.90 | 78.86 | 76.80 | 218.13 | 78.91 |
4 | 47.25 | 38.86 | 38.83 | 41.89 | 47.35 | 38.85 |
5 | 54.86 | 55.28 | 55.21 | 49.90 | 54.95 | 55.24 |
6 | 19.64 | 18.28 | 18.22 | 18.44 | 19.70 | 18.28 |
7 | 33.62 | 34.28 | 34.20 | 34.04 | 33.59 | 34.17 |
8 | 40.65 | 40.65 | 40.67 | 40.82 | 40.81 | 40.72 |
9 | 49.83 | 50.36 | 50.31 | 50.36 | 49.82 | 50.25 |
10 | 36.86 | 37.20 | 37.15 | 37.04 | 36.91 | 37.16 |
11 | 21.50 | 20.96 | 20.75 | 21.37 | 21.50 | 20.89 |
12 | 25.15 | 27.27 | 27.51 | 26.62 | 25.18 | 27.31 |
13 | 37.73 | 36.63 | 37.24 | 37.95 | 38.20 | 37.01 |
14 | 41.93 | 41.80 | 42.29 | 42.80 | 42.92 | 42.66 |
15 | 26.86 | 26.79 | 28.98 | 27.39 | 27.45 | 27.17 |
16 | 33.13 | 32.85 | 28.73 | 35.43 | 35.54 | 34.96 |
17 | 80.17 | 80.29 | 59.27 | 43.00 | 43.02 | 43.05 |
18 | 48.30 | 49.17 | 47.97 | 48.85 | 48.27 | 49.68 |
19 | 48.03 | 52.25 | 51.06 | 43.79 | 47.98 | 52.61 |
20 | 149.64 | 212.20 | 211.78 | 154.73 | 150.59 | 212.91 |
21 | 29.39 | 27.55 | 27.64 | 31.75 | 29.86 | 27.64 |
22 | 38.47 | 38.70 | 32.42 | 39.83 | 39.99 | 39.84 |
23 | 26.63 | 27.99 | 27.96 | 72.11 | 26.67 | 27.97 |
24 | 21.00 | 15.38 | 15.36 | 11.23 | 21.05 | 15.37 |
25 | 16.04 | 16.17 | 16.13 | 16.46 | 15.98 | 16.07 |
26 | 15.90 | 16.03 | 15.82 | 16.00 | 15.81 | 15.90 |
27 | 13.76 | 13.17 | 14.23 | 14.56 | 14.50 | 14.46 |
28 | 206.08 | 17.70 | 18.03 | 17.97 | ||
29 | 109.65 | 29.94 | 30.23 | 106.82 | 109.40 | 29.17 |
30 | 19.28 | 65.01 | 19.33 |
The assignments were based on 1H-1H COSY, HMQC and HMBC experiments.