Table 2. Structure solution and refinement based on ADT data for 9,9′-bianthracene-10-carbo­nitrile (CNBA), tri-p-benzamide (OPBA3) and carbamazepine (CBMZ).

CBMZ1 and CBMZ2 are solved structures using EDT from van Genderen et al. (2016 ▸) using a Timepix ASIC detector (software: Amsterdam scientific instruments, Netherlands) and Jones et al. (2018 ▸) using Ceta CMOS (Thermo Fisher) detector. Measurement conditions indicate the use of sample cooling (RT: room temperature; LT: liquid nitro­gen cooling) and the used detector.

Sample	Chemical formula	Space group	Lateral crystal size (nm)	Measurement conditions	Tilt range (°)	No. of reflections measured, independent	Completeness (%)	R int, R solution (@res)†	R 1(@res)‡
CNBA	C29N1	P21/c	700 × 700	RT CCD	120	9415, 3519	87	21.8, 24.4 (8)	39.0 (8)
OPBA3	C18O6N3H15	P21/c	500 × 1000	RT CCD	120	9185, 3078	81	34.6 (10)	58.0 (10)
CBMZ	C15N2OH12	P21/n	150 × 100	LT CCD	97	5495, 3588	89	15.9, 26.8 (8)	43.6 (6)
CBMZ1	C15N2OH12	P21/n	1200 × 800	RT ASIC	51	2202, 1071	45	35.8, – (0.8)	28
CBMZ2	C15N2OH12	P21/n	700 × 1600	LT CMOS	140	4682, 1044	88	19.5, – (1.0)	19.3

^†Burla et al. (2015 ▸).

^‡Sheldrick (1997 ▸, 2015 ▸).