Table 2. Experimental details.

Crystal data
Chemical formula	C11H8O5·C2H6OS
M r	298.30
Crystal system, space group	Monoclinic, P21/c
Temperature (K)	293
a, b, c (Å)	23.1461 (12), 8.2631 (4), 14.6374 (8)
β (°)	97.687 (4)
V (Å3)	2774.4 (2)
Z	8
Radiation type	Mo Kα
μ (mm−1)	0.26
Crystal size (mm)	0.25 × 0.18 × 0.12
Data collection
Diffractometer	Bruker Kappa APEXII CCD
Absorption correction	Multi-scan (SADABS; Bruker, 2008 ▸)
T min, T max	0.742, 0.852
No. of measured, independent and observed [I > 2σ(I)] reflections	25798, 6824, 2743
R int	0.119
(sin θ/λ)max (Å−1)	0.666
Refinement
R[F 2 > 2σ(F 2)], wR(F 2), S	0.063, 0.208, 0.87
No. of reflections	6824
No. of parameters	376
H-atom treatment	H-atom parameters constrained
Δρmax, Δρmin (e Å−3)	0.69, −0.42

Computer programs: APEX2 and SAINT (Bruker, 2008 ▸), SHELXS2018 (Sheldrick, 2008 ▸), SHELXL2018 (Sheldrick, 2015 ▸), ORTEP-3 for Windows and Mercury (Macrae et al., 2008 ▸), WinGX (Farrugia, 2012 ▸); Mercury (Macrae et al., 2008 ▸), publCIF (Westrip, 2010 ▸) and PLATON (Spek, 2009 ▸).