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. 2019 Aug 12;10:3632. doi: 10.1038/s41467-019-11565-3

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© The Author(s) 2019

Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license, and indicate if changes were made. The images or other third party material in this article are included in the article’s Creative Commons license, unless indicated otherwise in a credit line to the material. If material is not included in the article’s Creative Commons license and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this license, visit http://creativecommons.org/licenses/by/4.0/.

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Fig. 3 — Analysis of n-butane adsorption energetics. in situ calorimetric analysis in parallel to adsorption/desorption of n-butane at 303 K for a DUT-46, b DUT-49, c DUT-50, and d DUT-151int. Adsorption and desorption in closed and open symbols, respectively, adsorption enthalpies red, enthalpy of desorption blue, error regimes indicated as coloured areas. e, f Adsorption enthalpies plotted against adsorbed amount of n-butane for the series non-interpenetrated MOFs (e) and in comparison with DUT-151int (f)