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. Author manuscript; available in PMC: 2019 Aug 13.
Published in final edited form as: Anal Bioanal Chem. 2018 Nov 28;411(3):669–678. doi: 10.1007/s00216-018-1481-0

Table 3.

Detection frequency, median, and concentration range for DEET and neonicotinoid biomarkers measured in 60 anonymous adult volunteers

Analyte Detection frequency (%) Median (μg/L) Range (μg/L)
Acetamiprid 2 <LOD <LOD–0.14
N-Desmethyl-acetamiprid 90 0.17 <LOD–2.2
Clothianidin 37 <LOD <LOD–2.2
DCBA 95 4.0 <LOD–433
Imidacloprid 30 <LOD <LOD–0.98
ECBA 83 0.92 <LOD–142
5-Hydroxy-imidacloprid 42 <LOD <LOD–9.2
Thiacloprid 0 NA NA

Limit of detection (LOD) in μg/L: acetamiprid and clothianidin = 0.1; N-desmethyl-acetamiprid and 5-hydroxyimidacloprid= 0.03; imidacloprid and ECBA = 0.05; DCBA = 0.06; and thiacloprid = 0.01 NA, not applicable