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Synthesis of C-modified desmuramyl peptides. Reagents and conditions: a) H2, 10% Pd/C, MeOH, 38 psi, rt, 24 h, 96%; b) adamant-1-ylamine hydrochloride, EDC·HCl, HOBt·H2O, Et3N, DCM/dioxane 1:1, 0 °C → rt, 48 h, 60%; c) TFA/DCM 1:2, rt, 1 h, quantitative.
