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. 2019 Jul 24;12(15):2353. doi: 10.3390/ma12152353

Figure 1.

Figure 1

(a) Schematic of the used vertical physical vapor transport (PVT) reactor on the left and the hot zone on the right. Starting from the bottom of the hot zone, a tantalum foil is introduced as a carbon getter. On top, a polycrystalline SiC source is placed. The spacer limits the source-to-substrate distance. The final part is the self-manufactured seeding stack. (b) The manufacturing process for the seeding stack is necessary for high-temperature growth. The starting material is epitaxial 3C-SiC-on-Si grown by chemical vapor deposition (CVD). The removal of the silicon substrate is performed using wet-chemical etching by HNA (HF:HNO3:H2O) resulting in a high-quality growth front and a low-quality transition side. The final merging process is performed with a carbon glue layer (black), homogeneous pressure and a specific temperature treatment.