. Author manuscript; available in PMC: 2020 Oct 1.

Published in final edited form as: J Mech Behav Biomed Mater. 2019 Jun 10;98:90–95. doi: 10.1016/j.jmbbm.2019.06.009

Table 2 -.

Means (SD) of the viscosity (η, Pa.s) for the liquid component modified with the HDDMA and/or thiourethane, and dynamic properties of polymerized bars: glass transition temperature (Tg, °C), breadth of tan delta (width at half-height, °C) and crosslinking density (mog/kg). Different HDDMA concentrations were added to materials without (0 wt%) or with (10 wt%) thiourethane oligomer. Values followed by the same letters in each column are statistically similar (α=0.05).

TU wt%	HDDMA wt%	Viscosity (η, Pa.s× 10⁻⁴)	Glass transition temperature (Tg, °C)	Width at half-height of tan delta peak (°C)	Crosslinking density at 180°C (mol/kg × 10⁻⁴)
0	0	10.6 (8.6)a	138.5 (8.8)ab	29.94 (0.61)b	1.89 (0.15)b
	10	3.4 (0.0)b	144.5 (1.0)a	29.94 (1.25)b	2.02 (0.09)ab
	20	3.5 (0.0)b	146.8 (1.4)a	32.40 (0.26)b	2.26 (0.11)a
	30	3.5 (0.0)b	145.7 (0.5)a	31.69 (0.5l)b	2.29 (0.17)a
10	0	9.4 (1.0)a	121.9 (1.42)c	45.89 (1.14)a	1.13 (0.09)d
	10	3.5 (0.0)b	128.2 (2.6)bc	43.49 (0.02)a	1.74 (0.40)c
	20	4.8 (2.2)b	125.5 (0.8)c	47.32 (0.1 l)a	1.88 (0.01)bc
	30	3.5 (0.0)b	134.6 (2.2)b	45.04 (0.67)a	1.89 (0.07)bc

TU (Thio-urethane).

^**

HDDMA (1.6-Hexanediol dimethacrylate).