Table 1.
Data collection and refinement statistics
| GFLD·Cu | |
|---|---|
| Data collection | |
| Space group | P212121 |
| Cell dimensions | |
| a, b, c (Å) | 34.05, 49.07, 66.16 |
| Resolution (Å)a | 30.28–1.75 (1.81–1.75) |
| Rsym | 6.3 (42.9) |
| I/σI | 12.99 (3.19) |
| Completeness (%) | 99.85 (100.00) |
| Redundancy | 5.9 (6.0) |
| Refinement | |
| Resolution (Å) | 30.28–1.75 (1.81–1.75) |
| n reflections | 11674 |
| Rwork/Rfree | 0.1807/0.2303 |
| n atoms | |
| Protein/ligand/water | 826/7/52 |
| B-factors | |
| Protein/ligand/water | 44.8/52.8/53.9 |
| rms deviations | |
| Bond lengths (Å) | 0.007 |
| Bond angles (°) | 1.16 |
Values in parentheses are for the highest resolution shell.
aData measured on one crystal.