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. 2019 Aug 28;75(Pt 9):608–615. doi: 10.1107/S2053230X19011154

Table 3. Data collection and processing.

Values in parentheses are for the highest resolution shell.

Diffraction source SER-CAT beamline 22-BM, Advanced Photon Source
Wavelength (Å) 1.0000
Temperature (K) 100
Detector Rayonix MX300-HS
Crystal-to-detector distance (mm) 150
Rotation range per image (°) 1.0
Total rotation range (°) 180
Exposure per image (s) 3
Space group P212121
a, b, c (Å) 92.2, 99.4, 128.7
α, β, γ (°) 90.0, 90.0, 90.0
Mosaicity (°) 0.7
Resolution range (Å) 50–2.17 (2.21–2.17)
Total No. of reflections 279773
No. of unique reflections 61347 (3056)
Completeness (%) 97.6 (99.1)
Multiplicity 4.6 (4.2)
Mean I/σ(I) 17.1 (2.1)
R merge 0.050 (0.519)
R p.i.m. 0.041 (0.343)
CC1/2 0.996 (0.773)
Overall B factor from Wilson plot (Å2) 29