Table 4. Structure solution and refinement.
Values in parentheses are for the highest resolution shell.
| Resolution range (Å) | 26.71–2.17 (2.23–2.17) |
| No. of reflections used | 61296 |
| Final R work | 0.177 (0.227) |
| Final R free | 0.241 (0.332) |
| No. of non-H atoms | |
| Protein, total | 8680 |
| Protein, chain A | 2175 |
| Protein, chain B | 2169 |
| Protein, chain C | 2182 |
| Protein, chain D | 2154 |
| Water | 623 |
| Ethylene glycol | 8 |
| Estimated coordinate error (Å) | 0.26 |
| R.m.s. deviations | |
| Bond lengths (Å) | 0.008 |
| Bond angles (°) | 0.9 |
| Average B factors (Å2) | |
| Protein chain A | 33 |
| Protein chain B | 34 |
| Protein chain C | 38 |
| Protein chain D | 38 |
| All protein chains | 36 |
| Water | 37 |
| Ethylene glycol | 37 |
| Ramachandran plot | |
| Favored (%) | 96.2 |
| Allowed (%) | 3.4 |
| Outliers (%) | 0.4 |
| PDB code | 6mnu |