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. 2019 Jul 25;8(8):243. doi: 10.3390/antiox8080243

Table 1.

Chemical composition of thyme waste extract. Total polyphenols content and DPPH activity of thyme waste extract.

No. Retention Time RT (time) Relative Area Percent (%) Compounds m/z (I)
1 7.05 40.88 Benzoic acid 105(100); 179(93); 77(93); 135(82); 51(22); 180(13); 136(11); 73(8); 106(7); 75(7)
2 10.93 11.89 trans-Cinnamic acid (TMS) 131(100); 205(95); 103(95); 161(85); 77(74); 75(75); 145(45); 102(43); 135(25); 73(24)
3 11.83 17.18 4-Hydroxybenzoic acid (2TMS) 73(100); 267(72); 223(68); 193(46); 268(16); 224(15); 282(14); 75(12); 126(10); 91(10)
4 15.16 10.34 p-Coumaric acid (TMS) 73(100); 293(43); 219(40); 75(30); 249(30); 308(24); 179(11); 294 (10); 74(10); 220(8)
5 16.40 2.55 Ferulic acid (2TMS) 73(100); 338(45); 323(20); 75(34); 308(34); 249(30); 293(30); 59 (13); 219(13); 339(12)
6 16.70 8.74 Caffeic acid (TMS) 73(100); 219(68); 396(38); 191(16); 381(13); 397 (13); 220(12); 75(11); 74(8); 249(7)
7 17.37 3.71 Sinapic acid (2TMS) 73(100); 338(57); 368(45); 75(34); 353(32); 232(25); 279(15); 339(15); 59(14); 249(12)
8 21.91 0.90 Quercetin (5TMS) 73(100); 647(29); 648(16); 649(9); 559(8); 74(7); 75(6); 560(3); 147(3); 575(2)
Total * 96.19
* Only the most abundant peaks were identified.
I: intensity
Phenols (mg EAG/g) Flavones (mg EQ/g) Dihydroflavonols (mg EE/g) DPPH (IC50 mg/mL)
97.50 ± 3.82 0.13 ± 0.01 1.76 ± 0.24 0.093 ± 0.01