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(a) TGA curves of unmodified ACC (black line) and hybrid PAni-ACC composites synthesized after 40 min (red line) and 120 min (blue line) of galvanostatic electropolymerization; the inset shows the thermal pattern during the first thermogravimetric run up to 120 °C; the main panel shows the thermal behavior of the resulting dried samples; (b) Evolution of the total weight loss at 1000 °C for heat-dried PAni-ACC composites obtained at different electropolymerization times.
