Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C17H16O4 |
| M r | 284.30 |
| Crystal system, space group | Monoclinic, P21/n |
| Temperature (K) | 296 |
| a, b, c (Å) | 12.0914 (8), 9.4741 (6), 12.7761 (9) |
| β (°) | 92.943 (4) |
| V (Å3) | 1461.64 (17) |
| Z | 4 |
| Radiation type | Cu Kα |
| μ (mm−1) | 0.75 |
| Crystal size (mm) | 0.26 × 0.22 × 0.18 |
| Data collection | |
| Diffractometer | Bruker D8 Venture/Photon 100 CMOS |
| Absorption correction | Multi-scan (SADABS; Krause et al., 2015 ▸) |
| T min, T max | 0.654, 0.754 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 7496, 2996, 1972 |
| R int | 0.038 |
| (sin θ/λ)max (Å−1) | 0.637 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.048, 0.136, 1.03 |
| No. of reflections | 2996 |
| No. of parameters | 193 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.17, −0.16 |