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Plot of [n-C8H17N(i-Pr)2]/[1-octene] versus [THF] in hexane for the reaction of triflate 13 with 0.10 M NaDA at −78 °C (eq 13). The curve depicts an unweighted least-squares fit to the function f(x) = k[THF] + k′ (k = 0.33 ± 0.03; k′= 2.4 ± 0.2).
