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. Author manuscript; available in PMC: 2020 Sep 11.
Published in final edited form as: J Am Chem Soc. 2019 Aug 29;141(36):14136–14141. doi: 10.1021/jacs.9b08715

Figure 2.

Figure 2.

Product formation as monitored by 1H NMR analysis in reactions conducted using the “different excess” protocol: [Ir] = 0.01 M; [KH2PO4] = 0.2 M. (left) [2a]0 = 0.2 M, [1]0 = as noted; (middle) [1]0 = 0.3 M, [2a]0 = as noted. (right) Product formation varying catalyst loading reactions as monitored by NMR analysis: [1] = 0.3 M; [2a] = 0.2 M; [KH2PO4] = 0.2 M; [cat] = as noted.