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. Author manuscript; available in PMC: 2020 Sep 11.
Published in final edited form as: J Am Chem Soc. 2019 Aug 29;141(36):14136–14141. doi: 10.1021/jacs.9b08715

Table 1.

Selected optimization experiments in the enantioselective iridium-catalyzed (α-amino)allylation of phthalimido-allene 1 with alcohol 2a.a

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a

Yields are of material isolated by silica gel chromatography. Diastereoselectivities were determined by 1H NMR of crude reaction mixtures. Enantioselectivities were determined by chiral stationary phase HPLC analysis. See Supporting Information for experimental details.