Scheme 2. Scope of Semiheterogeneous Thioetherification.
Reaction conditions: methyl 4-iodobenzoate (1.2 mmol), thiol (2.4 mmol), CN-OA-m (20 mg), NiBr2·3H2O (120 μmol), dtbbpy (120 μmol), BIPA (6.0 mmol), MeCN (6.0 mL), white LEDs at 40 °C.
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