Table 1.
Data collection and refinement statistics
| OTULINcat–SNX27PDZ | |
|---|---|
| Data collection | |
| Beamline | Diamond I03 |
| Space group | P 1 |
| a, b, c (Å) | 54.65, 62.92, 72.02 |
| α, β, γ (°) | 65.13, 85.98, 85.38 |
| Wavelength (Å) | 0.96861 |
| Resolution (Å) | 42.65–2.00 (2.05–2.00) |
| R merge | 8.8 (53.1) |
| <I / σI > | 5.7 (1.8) |
| CC (1/2) | 0.99 (0.38) |
| Completeness (%) | 95.6 (94.2) |
| Redundancy | 1.7 (1.8) |
| Refinement | |
| Resolution (Å) | 42.66–2.00 |
| No. reflections | 55,971 |
| Rwork/Rfree | 21.5/25.3 |
| No. atoms | |
| Protein | 5674 |
| Ligand / ion | 84 |
| Water | 268 |
| B-factors | |
| Wilson B | 34.01 |
| Protein | 52.63 |
| Ligand/ion | 88.02 |
| Water | 59.9 |
| R.m.s. deviations | |
| Bond length (Å) | 0.003 |
| Angels (°) | 0.581 |
| Ramachandran statistics (outliers, allowed, favored) | 0.0, 2.5, 97.5 |
Numbers in parentheses are for the highest resolution bin