Table 3.
Crystallographic data for N-(pyridin-2-yl)hydrazinecarbothioamide
| N-(pyridin-2-yl)hydrazinecarbothioamide | |
|---|---|
| Formula | C6H8N4S |
| Formula weight | 168.22 |
| Temperature/K | 293 |
| Crystal system | Monoclinic |
| Space group | C2/c |
| Lattice parameters | |
| a/Å | 15.5906 (7) |
| b/Å | 10.1719 (5) |
| c/Å | 11.1763 (6) |
| α/° | 90.00 |
| β/° | 121.116 (3) |
| γ/° | 90.00 |
| V/Å3 | 1517.39 (13) |
| Z | 8 |
| Dcalc/g/cm3 | 1.473 |
| F 000 | 704 |
| μMo-Kα Å | 0.71073 |
| Reflections collected | 7055 |
| Independent reflections | 2200 |
| Data/parameters/restrains | 2200/100/0 |
| Goodness of fit on F2 | 1.041 |
| Absorption coefficient mm−1 | 0.36 |
| Final R indices (I > 2.00σ(I)) | R1 = 0.0602, wR2 = 0.1649 |
| R indices (all data) | R1 = 0.1385, wR2 = 0.1965 |
| Maximum/minimum residual electron density (e. Å−3) | 0.397/− 0.489 |