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. 2019 Sep 12;9(9):478. doi: 10.3390/biom9090478

Table 7.

Identified compounds from the extracts of D. crepidatum by GC–MS. RT—retention time.

RT (min) Compound Name Peak Area Percentage in the Extract
DCH DCC DCA DCE DCM
4.060 Dimethylsulfoxonium formylmethylide 7.15 14.94
4.253 2-Phenylethanol 0.94
4.261 1-Butoxy-2-propanol acetate 4.14
4.340 2,3-dihydro-3,5-dihydroxy-6-methyl-4H-Pyran-4-one 5.21 13.60
4.375 2,5-Dimethyl-4-hydroxy-3(2H)-furanone 4.56
4.585 (l)-alpha-Terpineol 1.12
4.652 (−)-alpha-Terpineol 0.86
4.806 2-Furaldehyde 5.78
5.217 5-(Hydroxymethyl)- 2-Furancarboxaldehyde 21.90 1.39
5.282 2-Methoxy-4-vinylphenol 0.84 2.22
5.430 4-methyl-1-naphthalenol 0.40 0.99
5.458 4-Methyl-1-naphthol 0.97 1.20
5.528 Eugenol 1.05
5.672 2-Methoxy-5-(1-propenyl)- phenol 0.79
6.286 N,N’-Dibutylidene-hydrazine 0.46
6.768 p-Mesyloxyphenol 0.49
7.285 , 2,6-Dimethoxy-4-(2-propenyl)-phenol 1.08
7.362 1,7-Trimethylene-2,3,5-trimethylindole 3.93
7.370 1-(3,4-Dihydro-1-naphthalenyl)- Pyrrolidine 4.22 1.04
7.495 3-(2-Phenylethylamino)-5-(4-methylphenyl)-2-cyclohexen-1-one 1.25
7.740 2-Benzylhexahydropyrrolizin-3-one 1.03 1.07
8.830 5-Acetyl-4-amino-3-(2-N-pyrrolidinylethylthio) thieno [3,2-d]isothiazole 2.58
8.841 2-t-Butyl-4-quinolinealdehyde 6.54
8.851 2,3-Dihydro-2,4,8-trimethyl-furo [2,3-b] quinoline 5.82 0.99
8.861 1,3,4,10-Tetrahydro-2-methyl-9(2H)-Acridinone 5.96
9.097 1,2-Benzenedicarboxylic acid, bis (2-methylpropyl) ester 2.05 1.38 1.19 16.08
9.099 Diisobutyl phthalate 3.73
9.547 4-Acetyl-3-amino-5-butyl-2,4-cyclopentadiene-1,1,2-tricarbonitrile 2.09 3.40
9.551 N-(N’-Ethoxycarbonylisonipecotinoyl)-isonipecotic acid ethyl ester 3.78
9.611 2,3,9-Trimethyl-5-trimethylsilyloxy-2-azabicyclodecane 1.44
9.680 2-Butoxy-5-(4-methylphenyl)- benzaldehyde 2.26
9.687 5,7-Dimethyl-9-hydroxy-2,3-dihydro-1H-cyclopenta [b] quinoline 3.45 4.30
9.724 7-Phenyl-1,5-dihydro-imidazo [4,5-d] pyridazin-4-one 1.64
9.733 Dibutyl phthalate 2.79
9.801 1-Heneicosanol 0.69
10.837 2,4-Dimethyl-3a-phenyldecahydrofuro[3,2-E] indolizin2-ol 5.23
11.191 1-Nonadecanol 1.10
11.415 9,12-Octadecadienoic acid, methyl ester 17.27
11.574 6-Isopentyl-2-tert-pentyl-tryptophan methyl ester 1.14
11.592 2-(1,1-Dimethylpropyl)-6-(3-methylbutyl)-tryptophan methyl ester 2.21 0.32
11.899 2-Dodecyl-5-methylpyrrolidine 1.60
11.997 Octahydro-2H-Inden-2-one, cis-oxime 1.44
12.175 5-sec-butylpyrogallol 5.54
12.187 1,2-Dihydro-2-(2-oxocyclohexylidene) quinoline 5.02
12.269 Isocrepidamine 2.80 2.28
12.326 1-(6-Hydroxy-7-methyl-6-phenyloctahydro-5-indolizinyl) acetone 3.73
12.438 1-Eicosanol, trifluoroacetate 0.70
12.728 2-(Diethylamino)-7-methyl-7phenyl-2,4-cycloheptadien-1-one 2.26
12.802 2,4-Cycloheptadien-1-one, 2-(diethylamino)-7-methyl-7-phenyl 2.37 0.36
12.915 3-Bornanone, oxime 1.89
12.931 3,12-Didehydro-9,10-dimethoxy-galanthan-1,2-diol 4.66
13.064 iso-Propyl 9-cis,11-trans-octadecadienoate 5.48
13.092 4-Methoxy-6-(1-pyrrolidinylmethyl)-1,3,5-triazin-2-amine 6.48
13.093 2-Hydrazino-6-methylpyrimidin-4-ol 7.01
13.125 Tetracosane 3.74
13.135 Crepidamine 3.79 10.17 4.50 1.43
13.139 9-Methoxy-9-Borabicyclo [3.3.1] nonane 1.32
13.190 Gephyrotoxin 207a 3.51 0.64
13.253 2-Methoxy-3-(1-methylpropyl)- pyrazine 3.14
13.399 1-(2-Hydroxy-3,4-dimethoxyphenyl)-2-(4-methoxyphenyl) ethanone 5.20
13.410 1-[2-(5-Hydroxy-1,1-dimethylhexyl)-3-methyl-2-cyclopropen-1-yl]-ethanone 2.93
13.464 N-(9H-Xanthen-9-yl)- 4-pyridinecarbothioamide 3.25
13.519 2-Hydroxy-3,4-dimethoxy-alpha-(p-methoxyphenyl) acetophenone 4.15 0.54
13.537 (−)-Nortrachelogenin 2.60
13.793 Heneicosane 1.25
13.942 Crepidine 3.19 4.87 7.08 0.37 0.56
14.041 Dimethoxymethylphenylsilane 3.30 1.75
14.544 n-Tetratriacontane 3.42
14.599 Tetratriacontane 8.10
14.767 Monolinolein 0.67
14.791 n-Propyl 9,12-octadecadienoate 3.01
14.913 cis-3,3,5-Trimethyl-cyclohexanol acetate 0.87
15.019 6-(6-Acetonyl-5-hydroxy-1,4-dimethyl-5-phenyl-2-piperidyl)-3-hexen-2-one 1.34
15.240 Hexatriacontane 0.90
15.796 Oxalic acid, di-(1-menthyl) ester 2.07
15.945 n-Hexatriacontane 1.22
15.960 Triacontane 2.65
16.050 1-Heptacosanol 1.44 0.75
17.611 gamma-Tocopherol 1.37
18.477 alpha-Tocopherol-beta-d-mannoside 2.19
19.908 (3beta)-ergost-5-en-3-ol 0.85
20.355 Stigmasterol 2.03
21.115 2-(1-methylimidazol-4-yl)-1,2,3,4-tetrahydroquinoline 7.44
21.159 1,2,3,4-Tetrahydro-2-(1-methylimidazol-4-yl)-quinoline 2.53 2.70
21.424 Estrone-3-acetate-17-methyloxime 3.98 1.05
23.109 dl-alpha-Tocopherol 2.66
24.466 3,4,5-Trimethoxy-nitrobenzene 0.60 1.69 2.62