Scheme 3.
Reaction scale‐up. Feed 1: 1 m (9.06 g, 60 mmol), Fe(acac)3 (423.6 mg, 2 mol %), THF (150 mL); feed 2: 2 b (150 mL, 1.0 m in THF, 2.5 equiv), SIPr⋅HCl, (1.02 g, 4 mol %); 25 °C, residence time: 5 min.
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