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. Author manuscript; available in PMC: 2020 Apr 10.
Published in final edited form as: J Am Chem Soc. 2019 Mar 26;141(14):5835–5855. doi: 10.1021/jacs.9b00097

Figure 6.

Figure 6.

Dependence of the initial rate (mM/min) for formation of product 26 on (a) [25]init (5–25 mM) with [MeMgI] = 0.50 M, and [catalyst] = 0.1 mM in toluene; (b) [catalyst] (0.1–1.0 mM) with [25] = 10 mM, and [MeMgI] = 50 mM in toluene; (c) [MeMgI] (2–10 mM) with [25] = 50 mM and [catalyst] = 0.5 mM in toluene; (d) added [MgI2] (0–6 mM) with [25] = 50 mM, [MeMgI] = 4 mM and [catalyst] = 0.5 mM in toluene.