Table 4.
Synthesis, characterization methods, characteristics and antiplasmodial activity assessment of metal nanoparticles
Items | Parameters | Categories | References |
---|---|---|---|
Mode of preparation | Part used for NPs synthesis | Leaves | [47–50, 52, 53, 57–60] |
Flowers | [53] | ||
Seeds | [55, 56, 60] | ||
Barks | [57] | ||
Whole organism | [61–63] | ||
Extraction solvent | Water | [47, 48, 50–60] | |
Tris–HCl buffer | [49] | ||
Main method of preparation | Washing, cutting, boiling, decantation, filtration | [47–56, 59] | |
Physico-chemical characterization of NPs | Plasmon resonance | UV–Vis | [47, 48, 50–63] |
Shape, size and size distribution | FESEM/SEM, EDX, EDAX | [47, 48, 50–56, 60–63] | |
HRTEM/TEM, SAED | [49, 51, 57–61, 63] | ||
Silver content | AAS | [49] | |
Interface NPs-metabolites | FTIR | [49, 51–53, 55–57, 59, 60, 62, 63] | |
Size distribution | DLS | [49, 59] | |
Structure-crystallinity | XRD | [47–57, 61] | |
Stability | Zeta potential | [47, 51, 53, 55] | |
Characteristics of NPs | Metal source | AgNO3 | [47–50, 52, 54–58, 61, 63] |
HAuCl4 | [53, 57, 60, 61] | ||
Pd(OAc)2 | [51] | ||
TiCl4 | [59] | ||
Time of production | < 30 min | [50, 58, 59, 61] | |
> 30 min | [47, 49, 51, 53–56] | ||
Shape | Spherical or mainly spherical | [47–51, 54, 56–59, 62] | |
Other shapes (cubical, polygonal, triangular, oval, ellipsoidal, rectangular) | [50–53, 55, 57–59, 61] | ||
NPs aggregation phenomenon | Yes | [49, 56] |
AAS atomic absorption spectroscopy, DLS dynamic light scattering, DRIFT diffuse reflectance infrared Fourier transform, EDS Electron Diffraction Spectrophotometer, FESEM field emission scanning electron microscopy, FTIR Fourier-transform infrared, HR-TEM high resolution transmission electron microscopy, SAED size and elected area diffraction, SEM scanning electron microscopy, TEM transmission electron microscopy, EDAX energy dispersive X-ray, HF health facility