| Oxford Diffraction Xcalibur with Sapphire CCD diffractometer | 4074 independent reflections |
| Radiation source: Enhance (Mo) X-ray Source | 2003 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.038 |
| ω scans | θmax = 28.0°, θmin = 2.7° |
| Absorption correction: multi-scan (CrysAlis RED; Oxford Diffraction, 2009) | h = −9→5 |
| Tmin = 0.916, Tmax = 0.993 | k = −9→9 |
| 8215 measured reflections | l = −42→41 |