| Oxford Diffraction Xcalibur with Sapphire CCD diffractometer | 2428 independent reflections |
| Radiation source: Enhance (Mo) X-ray Source | 2278 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.027 |
| ω scans | θmax = 27.7°, θmin = 3.0° |
| Absorption correction: multi-scan (CrysAlis RED; Oxford Diffraction, 2009) | h = −5→13 |
| Tmin = 0.476, Tmax = 0.892 | k = −16→17 |
| 6173 measured reflections | l = −14→5 |