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. 2019 Sep 20;75(Pt 10):1494–1506. doi: 10.1107/S2056989019012702
Oxford Diffraction Xcalibur with Sapphire CCD diffractometer 2428 independent reflections
Radiation source: Enhance (Mo) X-ray Source 2278 reflections with I > 2σ(I)
Graphite monochromator Rint = 0.027
ω scans θmax = 27.7°, θmin = 3.0°
Absorption correction: multi-scan (CrysAlis RED; Oxford Diffraction, 2009) h = −5→13
Tmin = 0.476, Tmax = 0.892 k = −16→17
6173 measured reflections l = −14→5