Oxford Diffraction Xcalibur with Sapphire CCD diffractometer	9650 independent reflections
Radiation source: Enhance (Mo) X-ray Source	7444 reflections with I > 2σ(I)
Graphite monochromator	θmax = 27.6°, θmin = 2.6°
ω scans	h = −11→11
Absorption correction: multi-scan (CrysAlis RED; Oxford Diffraction, 2009)	k = −19→19
Tmin = 0.892, Tmax = 0.947	l = −13→14
9650 measured reflections