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. 2019 Sep 20;75(Pt 10):1494–1506. doi: 10.1107/S2056989019012702
Oxford Diffraction Xcalibur with Sapphire CCD diffractometer 3477 independent reflections
Radiation source: Enhance (Mo) X-ray Source 1355 reflections with I > 2σ(I)
Graphite monochromator Rint = 0.046
ω scans θmax = 26.1°, θmin = 2.9°
Absorption correction: multi-scan (CrysAlis RED; Oxford Diffraction, 2009) h = −7→6
Tmin = 0.973, Tmax = 0.996 k = −9→9
5760 measured reflections l = −23→22