| Oxford Diffraction Xcalibur with Sapphire CCD diffractometer | 3454 independent reflections |
| Radiation source: Enhance (Mo) X-ray Source | 1343 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.041 |
| ω scans | θmax = 25.5°, θmin = 2.8° |
| Absorption correction: multi-scan (CrysAlis RED; Oxford Diffraction, 2009) | h = −7→7 |
| Tmin = 0.951, Tmax = 0.995 | k = −9→8 |
| 5883 measured reflections | l = −24→22 |