| Crystal data |
| Chemical formula |
[Sn(C6H5)3(C7H14NS2)] |
|
M
r
|
526.30 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
100 |
|
a, b, c (Å) |
9.7572 (1), 11.7030 (2), 11.7602 (2) |
| α, β, γ (°) |
74.419 (1), 80.114 (1), 67.285 (2) |
|
V (Å3) |
1189.71 (4) |
|
Z
|
2 |
| Radiation type |
Cu Kα |
| μ (mm−1) |
10.25 |
| Crystal size (mm) |
0.12 × 0.11 × 0.08 |
| |
| Data collection |
| Diffractometer |
Rigaku XtaLAB Synergy Dualflex AtlasS2 |
| Absorption correction |
Gaussian (CrysAlis PRO; Rigaku OD, 2018 ▸) |
|
T
min, T
max
|
0.840, 1.000 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
28219, 4248, 4231 |
|
R
int
|
0.022 |
| (sin θ/λ)max (Å−1) |
0.597 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.015, 0.040, 1.00 |
| No. of reflections |
4248 |
| No. of parameters |
266 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.36, −0.44 |
