Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C30H29NO |
| M r | 419.54 |
| Crystal system, space group | Orthorhombic, P212121 |
| Temperature (K) | 293 |
| a, b, c (Å) | 7.3009 (8), 11.0552 (11), 30.006 (3) |
| V (Å3) | 2421.8 (4) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.07 |
| Crystal size (mm) | 0.59 × 0.45 × 0.35 |
| Data collection | |
| Diffractometer | Nonius KappaCCD area detector |
| Absorption correction | Multi-scan (CrysAlis PRO; Rigaku OD, 2019 ▸) |
| T min, T max | 0.844, 1.000 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 21751, 4427, 3948 |
| R int | 0.027 |
| (sin θ/λ)max (Å−1) | 0.602 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.038, 0.083, 1.07 |
| No. of reflections | 4425 |
| No. of parameters | 295 |
| H-atom treatment | H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) | 0.11, −0.11 |
| Absolute structure | Refined as an inversion twin. |