Table 2. Experimental details.
| Crystal data | |
| Chemical formula | (C2H8N)2[Zn(C6H4O8P2)] |
| M r | 423.59 |
| Crystal system, space group | Monoclinic, P21/n |
| Temperature (K) | 220 |
| a, b, c (Å) | 8.8455 (5), 16.4492 (9), 11.2721 (6) |
| β (°) | 97.338 (1) |
| V (Å3) | 1626.67 (15) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 1.75 |
| Crystal size (mm) | 0.09 × 0.03 × 0.03 |
| Data collection | |
| Diffractometer | Bruker APEXII |
| Absorption correction | Multi-scan (SADABS; Krause et al., 2015 ▸) |
| T min, T max | 0.706, 0.746 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 19692, 4040, 3582 |
| R int | 0.027 |
| (sin θ/λ)max (Å−1) | 0.681 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.022, 0.060, 1.05 |
| No. of reflections | 4040 |
| No. of parameters | 288 |
| No. of restraints | 1 |
| H-atom treatment | All H-atom parameters refined |
| Δρmax, Δρmin (e Å−3) | 0.42, −0.31 |