| Crystal data |
| Chemical formula |
[Pt(C15H18N4O4S)(C2H6OS)] |
|
M
r
|
623.61 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
296 |
|
a, b, c (Å) |
6.5264 (3), 8.9024 (3), 18.9261 (7) |
| α, β, γ (°) |
82.228 (1), 87.074 (1), 74.739 (1) |
|
V (Å3) |
1050.96 (7) |
|
Z
|
2 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
6.91 |
| Crystal size (mm) |
0.49 × 0.21 × 0.15 |
| |
| Data collection |
| Diffractometer |
Bruker APEX Duo CCD area detector |
| Absorption correction |
Multi-scan (SADABS; Bruker, 2012 ▸) |
|
T
min, T
max
|
0.039, 0.092 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
41144, 6285, 5899 |
|
R
int
|
0.030 |
| (sin θ/λ)max (Å−1) |
0.711 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.019, 0.042, 1.09 |
| No. of reflections |
6285 |
| No. of parameters |
269 |
| H-atom treatment |
H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) |
0.98, −0.80 |
