Table 1. Crystallographic data and processing statistics.
Temperature (K) | 298 |
Exposure time (s) | 0.028 |
Space group | C121 |
a, b, c (Å) | 145.17, 100.15, 96.64 |
α, β, γ (°) | 90.0, 126.64, 90.0 |
No. of collected images | 214170 |
Average hit rate (%) | 4.7 |
No. of indexed images | 6513 |
Indexing rate (%) | 64.7 |
Total No. of reflections | 505407 |
No. of unique reflections | 27514 |
Multiplicity | 18 |
Completeness (%) | 100 (100) |
〈I/σ(I)〉 | 3 (1.3) |
Resolution range (Å) | 77.5–3.6 (3.66–3.60) |
R split | 0.31 (0.85) |
CC* | 0.89 (0.52) |
R work/R free (%) | 31.2/32.5 |