Table 1.
Entry | Conv. (%) 2 | Polyester (%) 2 | Mnexp 3 | PdI 3 |
---|---|---|---|---|
1 1 | 100 | 95 | 3572 | 1.11 |
2 4 | 100 | 94 | 3114 | 1.16 |
3 5 | 100 | 95 | 2533 | 1.21 |
4 6 | 100 | 98 | 2088 | 1.09 |
1 Reactions were carried out using [CHO]:[PA]:[Al]:[TBAB] = 200:200:1:1. 2 Determined by NMR. 3 Determined by GPC. 4 [CHO]:[PA]:[Al]:[TBAB] = 150:150:1:1. 5 [CHO]:[PA]:[Al]:[TBAB] = 100:100:1:1. 6 [CHO]:[PA]:[Al]:[TBAB] = 50:50:1:1.