. 2019 Sep 9;17(9):527. doi: 10.3390/md17090527

Table A13.

¹H chemical shifts (δ in ppm) of sulfates 44–46. Ref. = References.

Compounds	44	Compounds	45	46
Solvent	B	Solvent	B	B
Ref.	[15]	Ref.	[15]	[15]
Hydrogen	δ_H, m, J (Hz)
1	4.02 (m)	1 α	3.80 (dd, J = 6.6, 9.1)	3.79 (dd, J = 6.6, 9.4)
2α	1.42 ^a	1 β	3.88 (dd, J = 6.6, 9.1)	3.87 (dd, J = 6.6, 9.4)
2β	1.68 (m)	2	1.78 (m)	1.79 (m)
3	1.60 (m)	3	1.14 (m) 1.40 1.41 ^a	1.14 (m) 1.43 1.44 ^a
4	1.10 ^a 1.30 1.30 ^a	4	1.33 ^a	1.32 ^a
5	1.30 ^a	5	1.10 ^a 1.30 1.30 ^a	1.11 ^a 1.32 1.30 ^a
6α	1.10 ^a	6	1.39 ^a	1.41 ^a
6β	1.28 ^a	7	1.10 ^a 1.30 1.30 ^a	1.11 ^a 1.32 1.30 ^a
7	1.40 ^a	8	1.33 ^a	1.32 ^a
8α	1.09 ^a1.28	9	1.31 ^a 1.36 1.36 ^a	1.23 ^a 1.33 1.32 ^a
8β	1.28 ^a	10	1.66 (m)	1.44 (m)
9	1.29 ^a	11	1.30 ^a 1.38 1.38 ^a	1.23 ^a 1.33 1.32 ^a
10	1.30 ^a 1.38 1.38 ^a	12	1.33 ^a	1.33 ^a
11	1.65 (m)	13	1.42 ^a	1.19 (m)
12	1.36 ^a	14	-	1.55 (m)
13	1.30 ^a	15	1.15 (s)	0.89 (d, J = 6.4)
14	1.42 ^a	16	0.94 (d, J = 6.6)	0.96 (d, J = 6.6)
15	-	17	0.86 (d, J = 6.6)	0.88 (d, J = 6.4)
16	1.14 (s)	18	3.92 (d, J = 5.4)	3.44 (d, J = 5.4)
17	0.90 (d, J = 6.6)	19	1.15 (s)	0.89 (d, J = 6.4)
18	0.85 (d, J = 6.6)	-	-	3.79 (dd, J = 6.6, 9.4)
19	3.91 (d, J = 5.4)	-	-	3.87 (dd, J = 6.6, 9.4)
20	1.14 (s)	-	-	-

^a Signals overlapped by other resonances.