Table 1.
No. | 1 | 2 | ||
---|---|---|---|---|
δC, Type | δH, (J in Hz) | δC, Type | δH, (J in Hz) | |
1 | 161.8, C | 169.4, C | ||
2 | 116.3, C | 117.8, C | ||
3 | 127.4, CH | 7.75, dd (1.6, 7.7) | 131.2, CH | 7.99, d (8.3) |
4 | 117.9, CH | 6.85, m | 123.5, CH | 7.19, t (7.4) |
5 | 133.9, CH | 7.45, t (8.5) | 133.8, CH | 7.62, m |
6 | 112.5, CH | 6.85, m | 127.4, CH | 8.47, d (8.3) |
7 | 147.1, C | 140.0, C | ||
8 | ||||
9 | 42.1, CH2 | 3.76, d (16.4) 4.45, d (16.4) | 163.0, C | |
10 | 109.9, C | 122.4, C | ||
11 | 156.6, C | 129.5, CH | 7.76, d (8.7) | |
12 | 97.1, CH | 6.32, d (1.6) | 115.9, CH | 6.95, d (8.7) |
13 | 157.2, C | 161.9, C | ||
14 | 106.3, CH | 6.16, d (1.6) | 115.9, CH | 6.95, d (8.7) |
15 | 132.8, C | 129.5, CH | 7.76, d (8.7) | |
16 | 41.7, CH2 | 2.80, d (15.9) 3.08, d (15.9) | 12.09, d (10.6) | |
17 | 68.9, C | 137.4, CH | 7.64, m | |
18 | 8.42, s | 100.2, CH | 5.46, d (8.7) | |
19 | 21.3, CH3 | 1.20, s | 167.4, C | |
20 | 55.3, CH3 | 3.80, s | ||
13-OH | 9.40, s |