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. 2019 Sep 5;17(9):522. doi: 10.3390/md17090522

Table 1.

1H (400 MHz) and 13C (100 MHz) NMR data of 1 and 2 in DMSO-d6.

No. 1 2
δC, Type δH, (J in Hz) δC, Type δH, (J in Hz)
1 161.8, C 169.4, C
2 116.3, C 117.8, C
3 127.4, CH 7.75, dd (1.6, 7.7) 131.2, CH 7.99, d (8.3)
4 117.9, CH 6.85, m 123.5, CH 7.19, t (7.4)
5 133.9, CH 7.45, t (8.5) 133.8, CH 7.62, m
6 112.5, CH 6.85, m 127.4, CH 8.47, d (8.3)
7 147.1, C 140.0, C
8
9 42.1, CH2 3.76, d (16.4) 4.45, d (16.4) 163.0, C
10 109.9, C 122.4, C
11 156.6, C 129.5, CH 7.76, d (8.7)
12 97.1, CH 6.32, d (1.6) 115.9, CH 6.95, d (8.7)
13 157.2, C 161.9, C
14 106.3, CH 6.16, d (1.6) 115.9, CH 6.95, d (8.7)
15 132.8, C 129.5, CH 7.76, d (8.7)
16 41.7, CH2 2.80, d (15.9) 3.08, d (15.9) 12.09, d (10.6)
17 68.9, C 137.4, CH 7.64, m
18 8.42, s 100.2, CH 5.46, d (8.7)
19 21.3, CH3 1.20, s 167.4, C
20 55.3, CH3 3.80, s
13-OH 9.40, s