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. 2019 Oct 1;52(Pt 5):1189–1201. doi: 10.1107/S160057671901121X

Table 2. The standard equipment and relevant information required to plan an experiment at the instrument.

  Temperature range Time to cool/heat Sample holder Other
POWGEN auto changer (PAC) 10–300 K. 45 min to cool from 300 to 10 K. Specially designed V cans. 24 sample changer. The time for change is 8 min (Fig. 7).
 
Orange cryostat (Brochier, 1977) 2–300 K. 2 h to reach base temperature. PAC cans. Sample can be changed at 100 K.
 
Cryofurnace 5–500 K in cold stick. 30–750 K in hot stick. 2 h to cool from 750 to 300 K. 4 h to cool from 300 K to base temperature. PAC cans for cold stick and V cans with Ti flange lid for hot stick. Standard off-the-shelf closed-cycle refrigerator bought from Janis Research Company.
 
Vacuum and atmosphere furnaces (Niedziela et al., 2017) 300–1473 K with V heating element. 300–1873 K with Nb heating element. 4–5 h to cool from 1473 to 473 K. V can, BN lids and Mo screw. Nb peaks are observed in forward and backscattering detectors when Nb heating element is used. As a result, the Q range is reduced.
 
Vacuum and atmosphere furnaces with gas insert (Kirkham et al., 2018) 300–1123 K. 1.5 h to cool from 1123 to 473 K, with gas flow. Quartz basket with one open end and frit on the other end. Includes residual gas analyzer and pO2 sensor to measure the partial pressure of gas and detect incoming or outgoing gas. A wide variety of gasses are available. For specialized hazardous gas an additional review may be required.