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. 2019 Sep 16;11(9):539. doi: 10.3390/toxins11090539

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© 2019 by the authors.

Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (http://creativecommons.org/licenses/by/4.0/).

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The ¹H NMR spectra of synthetic 12β-deoxyGTX3 (3) and 12β-deoxyGTX2 (5) and observed key NOEs in these compounds. 600 MHz, solvent: CD₃COOD-D₂O (4:96, v/v). The HDO signal was suppressed. The signal of CHD₂COOD (2.06 ppm) was used as an internal reference.