Table 1.
Position | δC | type | δH, multiplicity (J = Hz) |
---|---|---|---|
1 | 171.0 | C | |
3 | 83.1 | CH | 4.48, brt (7.0) |
4 | 66.9 | CH | 4.73, brs |
4a | 135.0 | C | |
5 | 117.3 | CH | 7.20, s |
5a | 140.1 | C | |
6 | 99.1 | CH | 6.79, s |
7 | 161.7 | C | |
8 | 109.4 | C | |
9 | 155.6 | C | |
9a | 109.2 | C | |
10 | 163.1 | C | |
10a | 97.8 | C | |
11 | 28.0 | CH2 | 1.98, m |
12a | 32.0 | CH2 | 1.29, m |
12b | 1.65, m | ||
13 | 34.5 | CH | 1.42, m |
14 | 29.5 | CH2 | 1.22, m |
1.44, m | |||
15 | 11.5 | CH3 | 0.91, t (7.3) |
16 | 19.2 | CH3 | 0.94, d (6.5) |
17 | 56.2 | CH3 | 3.86, s |
4-OH | 1.86, brs | ||
9-OH | 9.67, s | ||
10-OH | 13.79, s |