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. 2019 Aug 22;12(18):4304–4312. doi: 10.1002/cssc.201901115

Table 1.

Comparison of data for thick juice to HMF reaction in batch and continuous setups.[a]

Entry

Setup

t [b]

[min]

pH

C NaCl

[mg mL−1]

X FRC [c]

[mol %]

S HMF [c, d]

[mol %]

1

batch

15

1.6

24.1

76.7

2

cont.

15

1.6

43.9

84.1

3

batch

30

1.6

51.2

81.7

4

cont.

30

1.6

65.8

87.4

5

batch

20

0.7

0.3

99.2

95.7

6

cont.

15

1.2

0.1

94.4

91.5

7

cont.

20

1.2

0.1

97.7

93.6

[a] Reactions performed at T=150 °C, H2O/MTHF ratio: 1:4 v/v, H2SO4 as acid catalyst. [b] Batch/residence time. [c] Determined by HPLC. [d] Based on FRC conversion.